Towards microfluidic reactors for in situ synchrotron infrared studies

I. P. Silverwood; N. Al-Rifai; E. Cao; D. J. Nelson; A. Chutia; P. P. Wells; S. P. Nolan; M. D. Frogley; G. Cinque; A. Gavriilidis; C. R. A. Catlow

doi:10.1063/1.4941825

Towards microfluidic reactors for in situ synchrotron infrared studies

I. P. Silverwood, N. Al-Rifai, E. Cao, D. J. Nelson, A. Chutia, P. P. Wells, S. P. Nolan, M. D. Frogley, G. Cinque, A. Gavriilidis, C. R. A. Catlow

Pure And Applied Chemistry

Research output: Contribution to journal › Article

3 Citations (Scopus)

Abstract

Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described

Language	English
Article number	024101
Number of pages	17
Journal	Review of Scientific Instruments
Volume	87
Early online date	19 Feb 2016
DOIs	10.1063/1.4941825
Publication status	E-pub ahead of print - 19 Feb 2016

Fingerprint

Synchrotrons

Microfluidics

synchrotrons

reactors

Infrared radiation

microfluidic devices

Silicon

Time measurement

time measurement

interference

probes

silicon

Temperature

Keywords

microfluidic devices
synchrotron
infrared
spectroscopic measurement
catalytic process
interference fringes

Cite this

Silverwood, I. P., Al-Rifai, N., Cao, E., Nelson, D. J., Chutia, A., Wells, P. P., ... Catlow, C. R. A. (2016). Towards microfluidic reactors for in situ synchrotron infrared studies. Review of Scientific Instruments, 87, [024101]. https://doi.org/10.1063/1.4941825

Silverwood, I. P. ; Al-Rifai, N. ; Cao, E. ; Nelson, D. J. ; Chutia, A. ; Wells, P. P. ; Nolan, S. P. ; Frogley, M. D. ; Cinque, G. ; Gavriilidis, A. ; Catlow, C. R. A. / Towards microfluidic reactors for in situ synchrotron infrared studies. In: Review of Scientific Instruments. 2016 ; Vol. 87.

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abstract = "Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described",

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Silverwood, IP, Al-Rifai, N, Cao, E, Nelson, DJ, Chutia, A, Wells, PP, Nolan, SP, Frogley, MD, Cinque, G, Gavriilidis, A & Catlow, CRA 2016, 'Towards microfluidic reactors for in situ synchrotron infrared studies' Review of Scientific Instruments, vol. 87, 024101. https://doi.org/10.1063/1.4941825

Towards microfluidic reactors for in situ synchrotron infrared studies. / Silverwood, I. P.; Al-Rifai, N.; Cao, E.; Nelson, D. J.; Chutia, A.; Wells, P. P.; Nolan, S. P.; Frogley, M. D.; Cinque, G.; Gavriilidis, A.; Catlow, C. R. A.

In: Review of Scientific Instruments, Vol. 87, 024101, 19.02.2016.

Research output: Contribution to journal › Article

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AU - Silverwood, I. P.

AU - Al-Rifai, N.

AU - Cao, E.

AU - Nelson, D. J.

AU - Chutia, A.

AU - Wells, P. P.

AU - Nolan, S. P.

AU - Frogley, M. D.

AU - Cinque, G.

AU - Gavriilidis, A.

AU - Catlow, C. R. A.

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KW - microfluidic devices

KW - synchrotron

KW - infrared

KW - spectroscopic measurement

KW - catalytic process

KW - interference fringes

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U2 - 10.1063/1.4941825

DO - 10.1063/1.4941825

M3 - Article

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