Towards microfluidic reactors for in situ synchrotron infrared studies

I. P. Silverwood; N. Al-Rifai; E. Cao; D. J. Nelson; A. Chutia; P. P. Wells; S. P. Nolan; M. D. Frogley; G. Cinque; A. Gavriilidis; C. R. A. Catlow

doi:10.1063/1.4941825

Towards microfluidic reactors for in situ synchrotron infrared studies

I. P. Silverwood, N. Al-Rifai, E. Cao, D. J. Nelson, A. Chutia, P. P. Wells, S. P. Nolan, M. D. Frogley, G. Cinque, A. Gavriilidis, C. R. A. Catlow

Pure And Applied Chemistry

Research output: Contribution to journal › Article

3 Citations (Scopus)

69 Downloads (Pure)

Abstract

Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described

Original language	English
Article number	024101
Number of pages	17
Journal	Review of Scientific Instruments
Volume	87
Early online date	19 Feb 2016
DOIs	https://doi.org/10.1063/1.4941825
Publication status	E-pub ahead of print - 19 Feb 2016

Fingerprint

Synchrotrons

Microfluidics

synchrotrons

reactors

Infrared radiation

microfluidic devices

Silicon

Time measurement

time measurement

interference

probes

silicon

Temperature

Keywords

microfluidic devices
synchrotron
infrared
spectroscopic measurement
catalytic process
interference fringes

Cite this

Silverwood, I. P., Al-Rifai, N., Cao, E., Nelson, D. J., Chutia, A., Wells, P. P., ... Catlow, C. R. A. (2016). Towards microfluidic reactors for in situ synchrotron infrared studies. Review of Scientific Instruments, 87, [024101]. https://doi.org/10.1063/1.4941825

Silverwood, I. P. ; Al-Rifai, N. ; Cao, E. ; Nelson, D. J. ; Chutia, A. ; Wells, P. P. ; Nolan, S. P. ; Frogley, M. D. ; Cinque, G. ; Gavriilidis, A. ; Catlow, C. R. A. / Towards microfluidic reactors for in situ synchrotron infrared studies. In: Review of Scientific Instruments. 2016 ; Vol. 87.

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abstract = "Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described",

keywords = "microfluidic devices, synchrotron, infrared, spectroscopic measurement, catalytic process, interference fringes",

author = "Silverwood, {I. P.} and N. Al-Rifai and E. Cao and Nelson, {D. J.} and A. Chutia and Wells, {P. P.} and Nolan, {S. P.} and Frogley, {M. D.} and G. Cinque and A. Gavriilidis and Catlow, {C. R. A.}",

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Silverwood, IP, Al-Rifai, N, Cao, E, Nelson, DJ, Chutia, A, Wells, PP, Nolan, SP, Frogley, MD, Cinque, G, Gavriilidis, A & Catlow, CRA 2016, 'Towards microfluidic reactors for in situ synchrotron infrared studies', Review of Scientific Instruments, vol. 87, 024101. https://doi.org/10.1063/1.4941825

Towards microfluidic reactors for in situ synchrotron infrared studies. / Silverwood, I. P.; Al-Rifai, N.; Cao, E.; Nelson, D. J.; Chutia, A.; Wells, P. P.; Nolan, S. P.; Frogley, M. D.; Cinque, G.; Gavriilidis, A.; Catlow, C. R. A.

In: Review of Scientific Instruments, Vol. 87, 024101, 19.02.2016.

Research output: Contribution to journal › Article

TY - JOUR

T1 - Towards microfluidic reactors for in situ synchrotron infrared studies

AU - Silverwood, I. P.

AU - Al-Rifai, N.

AU - Cao, E.

AU - Nelson, D. J.

AU - Chutia, A.

AU - Wells, P. P.

AU - Nolan, S. P.

AU - Frogley, M. D.

AU - Cinque, G.

AU - Gavriilidis, A.

AU - Catlow, C. R. A.

N1 - The following article has been submitted to/accepted by Review of Scientific Instruments. After it is published, it will be found at (http://scitation.aip.org/content/aip/journal/rsi).

PY - 2016/2/19

Y1 - 2016/2/19

N2 - Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described

AB - Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described

KW - microfluidic devices

KW - synchrotron

KW - infrared

KW - spectroscopic measurement

KW - catalytic process

KW - interference fringes

UR - http://scitation.aip.org/content/aip/journal/rsi

U2 - 10.1063/1.4941825

DO - 10.1063/1.4941825

M3 - Article

VL - 87

JO - Review of Scientific Instruments