Towards microfluidic reactors for in situ synchrotron infrared studies

I. P. Silverwood, N. Al-Rifai, E. Cao, D. J. Nelson, A. Chutia, P. P. Wells, S. P. Nolan, M. D. Frogley, G. Cinque, A. Gavriilidis, C. R. A. Catlow

Research output: Contribution to journalArticle

3 Citations (Scopus)

Abstract

Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described
LanguageEnglish
Article number024101
Number of pages17
JournalReview of Scientific Instruments
Volume87
Early online date19 Feb 2016
DOIs
Publication statusE-pub ahead of print - 19 Feb 2016

Fingerprint

Synchrotrons
Microfluidics
synchrotrons
reactors
Infrared radiation
microfluidic devices
Silicon
Time measurement
time measurement
interference
probes
silicon
Temperature

Keywords

  • microfluidic devices
  • synchrotron
  • infrared
  • spectroscopic measurement
  • catalytic process
  • interference fringes

Cite this

Silverwood, I. P., Al-Rifai, N., Cao, E., Nelson, D. J., Chutia, A., Wells, P. P., ... Catlow, C. R. A. (2016). Towards microfluidic reactors for in situ synchrotron infrared studies. Review of Scientific Instruments, 87, [024101]. https://doi.org/10.1063/1.4941825
Silverwood, I. P. ; Al-Rifai, N. ; Cao, E. ; Nelson, D. J. ; Chutia, A. ; Wells, P. P. ; Nolan, S. P. ; Frogley, M. D. ; Cinque, G. ; Gavriilidis, A. ; Catlow, C. R. A. / Towards microfluidic reactors for in situ synchrotron infrared studies. In: Review of Scientific Instruments. 2016 ; Vol. 87.
@article{58031e2c20214edab6c0f7ac35ce8a7d,
title = "Towards microfluidic reactors for in situ synchrotron infrared studies",
abstract = "Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described",
keywords = "microfluidic devices, synchrotron, infrared, spectroscopic measurement, catalytic process, interference fringes",
author = "Silverwood, {I. P.} and N. Al-Rifai and E. Cao and Nelson, {D. J.} and A. Chutia and Wells, {P. P.} and Nolan, {S. P.} and Frogley, {M. D.} and G. Cinque and A. Gavriilidis and Catlow, {C. R. A.}",
note = "The following article has been submitted to/accepted by Review of Scientific Instruments. After it is published, it will be found at (http://scitation.aip.org/content/aip/journal/rsi).",
year = "2016",
month = "2",
day = "19",
doi = "10.1063/1.4941825",
language = "English",
volume = "87",
journal = "Review of Scientific Instruments",
issn = "0034-6748",

}

Silverwood, IP, Al-Rifai, N, Cao, E, Nelson, DJ, Chutia, A, Wells, PP, Nolan, SP, Frogley, MD, Cinque, G, Gavriilidis, A & Catlow, CRA 2016, 'Towards microfluidic reactors for in situ synchrotron infrared studies' Review of Scientific Instruments, vol. 87, 024101. https://doi.org/10.1063/1.4941825

Towards microfluidic reactors for in situ synchrotron infrared studies. / Silverwood, I. P.; Al-Rifai, N.; Cao, E.; Nelson, D. J.; Chutia, A.; Wells, P. P.; Nolan, S. P.; Frogley, M. D.; Cinque, G.; Gavriilidis, A.; Catlow, C. R. A.

In: Review of Scientific Instruments, Vol. 87, 024101, 19.02.2016.

Research output: Contribution to journalArticle

TY - JOUR

T1 - Towards microfluidic reactors for in situ synchrotron infrared studies

AU - Silverwood, I. P.

AU - Al-Rifai, N.

AU - Cao, E.

AU - Nelson, D. J.

AU - Chutia, A.

AU - Wells, P. P.

AU - Nolan, S. P.

AU - Frogley, M. D.

AU - Cinque, G.

AU - Gavriilidis, A.

AU - Catlow, C. R. A.

N1 - The following article has been submitted to/accepted by Review of Scientific Instruments. After it is published, it will be found at (http://scitation.aip.org/content/aip/journal/rsi).

PY - 2016/2/19

Y1 - 2016/2/19

N2 - Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described

AB - Anodically bonded etched silicon microfluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described

KW - microfluidic devices

KW - synchrotron

KW - infrared

KW - spectroscopic measurement

KW - catalytic process

KW - interference fringes

UR - http://scitation.aip.org/content/aip/journal/rsi

U2 - 10.1063/1.4941825

DO - 10.1063/1.4941825

M3 - Article

VL - 87

JO - Review of Scientific Instruments

T2 - Review of Scientific Instruments

JF - Review of Scientific Instruments

SN - 0034-6748

M1 - 024101

ER -