Thermal volatilisation analysis - the development of a novel technique for the analysis of conservation artifacts

James Pawel Lewicki; Deborah Todd; Perrine Redon; John Liggat; Lorraine Gibson

doi:10.1557/PROC-1047-Y04-05

Thermal volatilisation analysis - the development of a novel technique for the analysis of conservation artifacts

James Pawel Lewicki, Deborah Todd, Perrine Redon, John Liggat, Lorraine Gibson

Pure And Applied Chemistry

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution book

2 Citations (Scopus)

Abstract

Reported here is the development of a novel evolved gas analysis technique: Sub-Ambient Thermal Volatilization Analysis (SATVA) and its application in characterizing key analyte species from conservation artifacts. In this work SATVA has been applied to the study of volatiles evolution processes occurring in number of model conservation artifacts. The evolution of volatile species from cured formaldehyde resin, leather and metallic artifacts has been studied by SATVA. The specific analytes making up the total quantity of evolved material in each case have been separated and identified using sub-ambient differential distillation and a combination of online mass spectrometry, gas phase IR spectroscopy and GC-MS. The data gathered has been used to provide information on both the degradation processes occurring within the artifacts and the environmental history of the artifacts themselves.

Original language	English
Title of host publication	Materials Research Society Symposium Proceedings - Materials Issues in Art and Archaeology VIII
Publisher	Cambridge University Press
Pages	307-318
Number of pages	12
Volume	1047
ISBN (Print)	9781558999886
DOIs	https://doi.org/10.1557/PROC-1047-Y04-05
Publication status	Published - 1 Dec 2008
Event	Materials Issues in Art and Archaeology VIII - Boston, MA, United States Duration: 26 Nov 2007 → 28 Nov 2007

Conference

Conference	Materials Issues in Art and Archaeology VIII
Country/Territory	United States
City	Boston, MA
Period	26/11/07 → 28/11/07

Keywords

analyte
analytes
degradation processes
environmental history
evolved gas analysis
gas-phase
Ir spectroscopies
on-line mass spectrometries
high performance liquid chromatography

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10.1557/PROC-1047-Y04-05

Cite this

Lewicki, J. P., Todd, D., Redon, P., Liggat, J., & Gibson, L. (2008). Thermal volatilisation analysis - the development of a novel technique for the analysis of conservation artifacts. In Materials Research Society Symposium Proceedings - Materials Issues in Art and Archaeology VIII (Vol. 1047, pp. 307-318). Cambridge University Press. https://doi.org/10.1557/PROC-1047-Y04-05

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abstract = "Reported here is the development of a novel evolved gas analysis technique: Sub-Ambient Thermal Volatilization Analysis (SATVA) and its application in characterizing key analyte species from conservation artifacts. In this work SATVA has been applied to the study of volatiles evolution processes occurring in number of model conservation artifacts. The evolution of volatile species from cured formaldehyde resin, leather and metallic artifacts has been studied by SATVA. The specific analytes making up the total quantity of evolved material in each case have been separated and identified using sub-ambient differential distillation and a combination of online mass spectrometry, gas phase IR spectroscopy and GC-MS. The data gathered has been used to provide information on both the degradation processes occurring within the artifacts and the environmental history of the artifacts themselves.",

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Lewicki, JP, Todd, D, Redon, P, Liggat, J & Gibson, L 2008, Thermal volatilisation analysis - the development of a novel technique for the analysis of conservation artifacts. in Materials Research Society Symposium Proceedings - Materials Issues in Art and Archaeology VIII. vol. 1047, Cambridge University Press, pp. 307-318, Materials Issues in Art and Archaeology VIII, Boston, MA, United States, 26/11/07. https://doi.org/10.1557/PROC-1047-Y04-05

Thermal volatilisation analysis - the development of a novel technique for the analysis of conservation artifacts. / Lewicki, James Pawel; Todd, Deborah; Redon, Perrine et al.
Materials Research Society Symposium Proceedings - Materials Issues in Art and Archaeology VIII. Vol. 1047 Cambridge University Press, 2008. p. 307-318.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution book

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N2 - Reported here is the development of a novel evolved gas analysis technique: Sub-Ambient Thermal Volatilization Analysis (SATVA) and its application in characterizing key analyte species from conservation artifacts. In this work SATVA has been applied to the study of volatiles evolution processes occurring in number of model conservation artifacts. The evolution of volatile species from cured formaldehyde resin, leather and metallic artifacts has been studied by SATVA. The specific analytes making up the total quantity of evolved material in each case have been separated and identified using sub-ambient differential distillation and a combination of online mass spectrometry, gas phase IR spectroscopy and GC-MS. The data gathered has been used to provide information on both the degradation processes occurring within the artifacts and the environmental history of the artifacts themselves.

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KW - analytes

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Thermal volatilisation analysis - the development of a novel technique for the analysis of conservation artifacts

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Keywords

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