The evolution of microstructure during thin slab direct rolling processing in vanadium microalloyed steel

Y. Li, D. Crowther, P.S. Mitchell, T.N. Baker

Research output: Contribution to journalArticle

48 Citations (Scopus)

Abstract

The evolution of microstructure during a simulation of the thin slab direct rolling process has been studied on two low carbon steels, microalloyed with V-N and V-Ti-N. The steels were examined using optical microscopy, analytical transmission electron microscopy (TEM) and energy dispersive X-ray (EDAX). After the 4th rolling pass, in a five pass schedule, the initial coarse austenite grain size (≈1 mm) was reduced to about 50 μm in Steel V-N and 22μm in Steel V-Ti-N. The average ferrite grain size in the final strip was slightly smaller in Steel V-Ti-N (4.8-6.6 μm) than in Steel V-N (5.3-7.2 μm). For Steel V-N, VN was only observed after 1 050°C equalization, but it was not found after 1 200°C and 1 100°C equalisation. For Steel V-Ti-N, V-Ti(N) particles formed during casting and during equalization for all the equalization temperatures (1 200°C, 1 100°C and 1 050°C). AlN particles precipitated in Steel V-N only during 1 050°C equalization and were often associated with MnS or MnS and VN. No AlN was detected in Steel V-Ti-N. Fine V containing precipitates (<10 nm) were observed in the final strip for both of the steels, but the frequency of the fine particles was lower in Steel V-Ti-N than in Steel V-N. The fine precipitates in the final strip make a major contribution to dispersion strengthening. High strength (LYS≈460-560 MPa) with good toughness and good ductility were achieved in the steels, which are competitive to similar products made by conventional controlled rolling. However, the addition of Ti to the V-N steel decreased the yield strength due to formation of V-Ti(N) particles in austenite, which reduced the amounts of V and N available for subsequent V rich fine particle precipitation in ferrite.
LanguageEnglish
Pages636-644
Number of pages8
JournalISIJ International
Volume42
Issue number6
DOIs
Publication statusPublished - 2002

Fingerprint

Vanadium
Steel
Microstructure
Processing
Austenite
Ferrite
Precipitates
Low carbon steel
Toughness
Optical microscopy
Yield stress
Ductility

Keywords

  • vanadium
  • vanadium-titanium
  • microalloyed steel
  • thin slab direct rolling
  • equalization temperature
  • microstructure

Cite this

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title = "The evolution of microstructure during thin slab direct rolling processing in vanadium microalloyed steel",
abstract = "The evolution of microstructure during a simulation of the thin slab direct rolling process has been studied on two low carbon steels, microalloyed with V-N and V-Ti-N. The steels were examined using optical microscopy, analytical transmission electron microscopy (TEM) and energy dispersive X-ray (EDAX). After the 4th rolling pass, in a five pass schedule, the initial coarse austenite grain size (≈1 mm) was reduced to about 50 μm in Steel V-N and 22μm in Steel V-Ti-N. The average ferrite grain size in the final strip was slightly smaller in Steel V-Ti-N (4.8-6.6 μm) than in Steel V-N (5.3-7.2 μm). For Steel V-N, VN was only observed after 1 050°C equalization, but it was not found after 1 200°C and 1 100°C equalisation. For Steel V-Ti-N, V-Ti(N) particles formed during casting and during equalization for all the equalization temperatures (1 200°C, 1 100°C and 1 050°C). AlN particles precipitated in Steel V-N only during 1 050°C equalization and were often associated with MnS or MnS and VN. No AlN was detected in Steel V-Ti-N. Fine V containing precipitates (<10 nm) were observed in the final strip for both of the steels, but the frequency of the fine particles was lower in Steel V-Ti-N than in Steel V-N. The fine precipitates in the final strip make a major contribution to dispersion strengthening. High strength (LYS≈460-560 MPa) with good toughness and good ductility were achieved in the steels, which are competitive to similar products made by conventional controlled rolling. However, the addition of Ti to the V-N steel decreased the yield strength due to formation of V-Ti(N) particles in austenite, which reduced the amounts of V and N available for subsequent V rich fine particle precipitation in ferrite.",
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author = "Y. Li and D. Crowther and P.S. Mitchell and T.N. Baker",
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The evolution of microstructure during thin slab direct rolling processing in vanadium microalloyed steel. / Li, Y.; Crowther, D.; Mitchell, P.S.; Baker, T.N.

In: ISIJ International, Vol. 42, No. 6, 2002, p. 636-644.

Research output: Contribution to journalArticle

TY - JOUR

T1 - The evolution of microstructure during thin slab direct rolling processing in vanadium microalloyed steel

AU - Li, Y.

AU - Crowther, D.

AU - Mitchell, P.S.

AU - Baker, T.N.

PY - 2002

Y1 - 2002

N2 - The evolution of microstructure during a simulation of the thin slab direct rolling process has been studied on two low carbon steels, microalloyed with V-N and V-Ti-N. The steels were examined using optical microscopy, analytical transmission electron microscopy (TEM) and energy dispersive X-ray (EDAX). After the 4th rolling pass, in a five pass schedule, the initial coarse austenite grain size (≈1 mm) was reduced to about 50 μm in Steel V-N and 22μm in Steel V-Ti-N. The average ferrite grain size in the final strip was slightly smaller in Steel V-Ti-N (4.8-6.6 μm) than in Steel V-N (5.3-7.2 μm). For Steel V-N, VN was only observed after 1 050°C equalization, but it was not found after 1 200°C and 1 100°C equalisation. For Steel V-Ti-N, V-Ti(N) particles formed during casting and during equalization for all the equalization temperatures (1 200°C, 1 100°C and 1 050°C). AlN particles precipitated in Steel V-N only during 1 050°C equalization and were often associated with MnS or MnS and VN. No AlN was detected in Steel V-Ti-N. Fine V containing precipitates (<10 nm) were observed in the final strip for both of the steels, but the frequency of the fine particles was lower in Steel V-Ti-N than in Steel V-N. The fine precipitates in the final strip make a major contribution to dispersion strengthening. High strength (LYS≈460-560 MPa) with good toughness and good ductility were achieved in the steels, which are competitive to similar products made by conventional controlled rolling. However, the addition of Ti to the V-N steel decreased the yield strength due to formation of V-Ti(N) particles in austenite, which reduced the amounts of V and N available for subsequent V rich fine particle precipitation in ferrite.

AB - The evolution of microstructure during a simulation of the thin slab direct rolling process has been studied on two low carbon steels, microalloyed with V-N and V-Ti-N. The steels were examined using optical microscopy, analytical transmission electron microscopy (TEM) and energy dispersive X-ray (EDAX). After the 4th rolling pass, in a five pass schedule, the initial coarse austenite grain size (≈1 mm) was reduced to about 50 μm in Steel V-N and 22μm in Steel V-Ti-N. The average ferrite grain size in the final strip was slightly smaller in Steel V-Ti-N (4.8-6.6 μm) than in Steel V-N (5.3-7.2 μm). For Steel V-N, VN was only observed after 1 050°C equalization, but it was not found after 1 200°C and 1 100°C equalisation. For Steel V-Ti-N, V-Ti(N) particles formed during casting and during equalization for all the equalization temperatures (1 200°C, 1 100°C and 1 050°C). AlN particles precipitated in Steel V-N only during 1 050°C equalization and were often associated with MnS or MnS and VN. No AlN was detected in Steel V-Ti-N. Fine V containing precipitates (<10 nm) were observed in the final strip for both of the steels, but the frequency of the fine particles was lower in Steel V-Ti-N than in Steel V-N. The fine precipitates in the final strip make a major contribution to dispersion strengthening. High strength (LYS≈460-560 MPa) with good toughness and good ductility were achieved in the steels, which are competitive to similar products made by conventional controlled rolling. However, the addition of Ti to the V-N steel decreased the yield strength due to formation of V-Ti(N) particles in austenite, which reduced the amounts of V and N available for subsequent V rich fine particle precipitation in ferrite.

KW - vanadium

KW - vanadium-titanium

KW - microalloyed steel

KW - thin slab direct rolling

KW - equalization temperature

KW - microstructure

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