Synthesis of oriented zeolite membranes at the interface between two fluid phases

V Tricoli, J Sefcik, A V McCormick

Research output: Contribution to journalLetter

11 Citations (Scopus)

Abstract

A method was developed for the synthesis of free-standing silicalite-1 membranes. Intergrown polycrystalline films were synthesized at the interface between a colloid-free aqueous phase and an organic phase or air. These films were characterized by scanning electron microscopy (SERI) and X-ray diffraction (XRD). It was found that the crystallites of the films formed at the air-water interface were oriented with their (010) axis orthogonal to the interface.

LanguageEnglish
Pages4193-4196
Number of pages4
JournalLangmuir
Volume13
Issue number16
DOIs
Publication statusPublished - 6 Aug 1997

Fingerprint

Zeolites
membranes
Membranes
Fluids
fluids
synthesis
air
Colloids
Air
Crystallites
crystallites
colloids
X ray diffraction
Scanning electron microscopy
scanning electron microscopy
Water
diffraction
water
x rays

Keywords

  • polycrystalline films
  • zeolite membranes

Cite this

Tricoli, V ; Sefcik, J ; McCormick, A V . / Synthesis of oriented zeolite membranes at the interface between two fluid phases. In: Langmuir. 1997 ; Vol. 13, No. 16. pp. 4193-4196.
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Synthesis of oriented zeolite membranes at the interface between two fluid phases. / Tricoli, V ; Sefcik, J ; McCormick, A V .

In: Langmuir, Vol. 13, No. 16, 06.08.1997, p. 4193-4196.

Research output: Contribution to journalLetter

TY - JOUR

T1 - Synthesis of oriented zeolite membranes at the interface between two fluid phases

AU - Tricoli, V

AU - Sefcik, J

AU - McCormick, A V

PY - 1997/8/6

Y1 - 1997/8/6

N2 - A method was developed for the synthesis of free-standing silicalite-1 membranes. Intergrown polycrystalline films were synthesized at the interface between a colloid-free aqueous phase and an organic phase or air. These films were characterized by scanning electron microscopy (SERI) and X-ray diffraction (XRD). It was found that the crystallites of the films formed at the air-water interface were oriented with their (010) axis orthogonal to the interface.

AB - A method was developed for the synthesis of free-standing silicalite-1 membranes. Intergrown polycrystalline films were synthesized at the interface between a colloid-free aqueous phase and an organic phase or air. These films were characterized by scanning electron microscopy (SERI) and X-ray diffraction (XRD). It was found that the crystallites of the films formed at the air-water interface were oriented with their (010) axis orthogonal to the interface.

KW - polycrystalline films

KW - zeolite membranes

U2 - 10.1021/la962095h

DO - 10.1021/la962095h

M3 - Letter

VL - 13

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EP - 4196

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T2 - Langmuir

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SN - 0743-7463

IS - 16

ER -