Pyrrolo[3,2,1-ij]quinolin-4-one and pyrrolo[3,2,1-ij]quinolin-6-one

Hamish McNab, David Nelson, Emma Rozgowska

Research output: Contribution to journalArticle

8 Citations (Scopus)

Abstract

The parent pyrrolo[3,2,1-ij]quinolin-4-one and pyrrolo[ 3,2,1-ij]quinolin-6-one ring systems were made by pyrolysis of appropriate acrylates. In the first case, the cyclisation was effected by flash vacuum pyrolysis (FVP) at 950 °C, in the second case a cyclisation-dehydrogenation was carried out in one step by FVP over a tungsten trioxide catalyst at 525 °C.

LanguageEnglish
Pages2171-2174
Number of pages4
JournalSynthesis
Volume13
DOIs
Publication statusPublished - 1 Jul 2009
Externally publishedYes

Fingerprint

Pyrolysis
Cyclization
Acrylates
Vacuum
Dehydrogenation
Tungsten
Catalysts
tungsten oxide

Keywords

  • pyrolysis
  • ketenes
  • gas
  • phase reactions
  • cyclisations
  • heterocycles

Cite this

McNab, Hamish ; Nelson, David ; Rozgowska, Emma. / Pyrrolo[3,2,1-ij]quinolin-4-one and pyrrolo[3,2,1-ij]quinolin-6-one. In: Synthesis. 2009 ; Vol. 13. pp. 2171-2174.
@article{116f2b65a64e47d3b40911224801d758,
title = "Pyrrolo[3,2,1-ij]quinolin-4-one and pyrrolo[3,2,1-ij]quinolin-6-one",
abstract = "The parent pyrrolo[3,2,1-ij]quinolin-4-one and pyrrolo[ 3,2,1-ij]quinolin-6-one ring systems were made by pyrolysis of appropriate acrylates. In the first case, the cyclisation was effected by flash vacuum pyrolysis (FVP) at 950 °C, in the second case a cyclisation-dehydrogenation was carried out in one step by FVP over a tungsten trioxide catalyst at 525 °C.",
keywords = "pyrolysis, ketenes, gas, phase reactions, cyclisations, heterocycles",
author = "Hamish McNab and David Nelson and Emma Rozgowska",
year = "2009",
month = "7",
day = "1",
doi = "10.1055/s-0029-1216858",
language = "English",
volume = "13",
pages = "2171--2174",
journal = "Synthesis",
issn = "0039-7881",
publisher = "Georg Thieme Verlag",

}

Pyrrolo[3,2,1-ij]quinolin-4-one and pyrrolo[3,2,1-ij]quinolin-6-one. / McNab, Hamish; Nelson, David; Rozgowska, Emma.

In: Synthesis, Vol. 13, 01.07.2009, p. 2171-2174.

Research output: Contribution to journalArticle

TY - JOUR

T1 - Pyrrolo[3,2,1-ij]quinolin-4-one and pyrrolo[3,2,1-ij]quinolin-6-one

AU - McNab, Hamish

AU - Nelson, David

AU - Rozgowska, Emma

PY - 2009/7/1

Y1 - 2009/7/1

N2 - The parent pyrrolo[3,2,1-ij]quinolin-4-one and pyrrolo[ 3,2,1-ij]quinolin-6-one ring systems were made by pyrolysis of appropriate acrylates. In the first case, the cyclisation was effected by flash vacuum pyrolysis (FVP) at 950 °C, in the second case a cyclisation-dehydrogenation was carried out in one step by FVP over a tungsten trioxide catalyst at 525 °C.

AB - The parent pyrrolo[3,2,1-ij]quinolin-4-one and pyrrolo[ 3,2,1-ij]quinolin-6-one ring systems were made by pyrolysis of appropriate acrylates. In the first case, the cyclisation was effected by flash vacuum pyrolysis (FVP) at 950 °C, in the second case a cyclisation-dehydrogenation was carried out in one step by FVP over a tungsten trioxide catalyst at 525 °C.

KW - pyrolysis

KW - ketenes

KW - gas

KW - phase reactions

KW - cyclisations

KW - heterocycles

UR - http://www.scopus.com/inward/record.url?scp=67651113411&partnerID=8YFLogxK

U2 - 10.1055/s-0029-1216858

DO - 10.1055/s-0029-1216858

M3 - Article

VL - 13

SP - 2171

EP - 2174

JO - Synthesis

T2 - Synthesis

JF - Synthesis

SN - 0039-7881

ER -