Modified dowex-50 W-promoted synthesis of chalcones containing hydroxyl and nitro groups

Ahmed A. H Al-Kadhimi; Abedawn I. Khalaf; Khalaid M. M Al-Janabi; Suad A. Jameel

doi:10.1016/j.kijoms.2014.12.001

Modified dowex-50 W-promoted synthesis of chalcones containing hydroxyl and nitro groups

Ahmed A. H Al-Kadhimi, Abedawn I. Khalaf, Khalaid M. M Al-Janabi, Suad A. Jameel

Pure And Applied Chemistry

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Abstract

Dowex-50W-sodium ion exchange was used after acidification and modification via nitration and sulfonation as a reusable catalyst for the synthesis of chalcones containing hydroxyl and nitro groups through condensation of substituted aldehydes and substituted acetophenone. This synthesis provides several advantages such as excellent yields of the required products. The prepared compounds (1-11) were identified by m.p., IR, CHN analysis, ¹H ND ¹³C-NMR

Original language	English
Journal	Karbala International Journal of Modern Science
Early online date	15 Dec 2014
DOIs	https://doi.org/10.1016/j.kijoms.2014.12.001
Publication status	Published - 2015

Keywords

Dowex resin
chalcones
Claisen-Schmidt condensation

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10.1016/j.kijoms.2014.12.001

Al-Kadhimi-etal-KIJOMS-2015-Modified-Dowes-50
Open Access funded by University of Kerbala
Accepted author manuscript, 1.01 MB

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title = "Modified dowex-50 W-promoted synthesis of chalcones containing hydroxyl and nitro groups",

abstract = "Dowex-50W-sodium ion exchange was used after acidification and modification via nitration and sulfonation as a reusable catalyst for the synthesis of chalcones containing hydroxyl and nitro groups through condensation of substituted aldehydes and substituted acetophenone. This synthesis provides several advantages such as excellent yields of the required products. The prepared compounds (1-11) were identified by m.p., IR, CHN analysis, 1H ND 13C-NMR",

keywords = "Dowex resin, chalcones, Claisen-Schmidt condensation",

author = "Al-Kadhimi, {Ahmed A. H} and Khalaf, {Abedawn I.} and Al-Janabi, {Khalaid M. M} and Jameel, {Suad A.}",

year = "2015",

doi = "10.1016/j.kijoms.2014.12.001",

language = "English",

journal = "Karbala International Journal of Modern Science",

publisher = "University of Kerbala",

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TY - JOUR

T1 - Modified dowex-50 W-promoted synthesis of chalcones containing hydroxyl and nitro groups

AU - Al-Kadhimi, Ahmed A. H

AU - Khalaf, Abedawn I.

AU - Al-Janabi, Khalaid M. M

AU - Jameel, Suad A.

PY - 2015

Y1 - 2015

N2 - Dowex-50W-sodium ion exchange was used after acidification and modification via nitration and sulfonation as a reusable catalyst for the synthesis of chalcones containing hydroxyl and nitro groups through condensation of substituted aldehydes and substituted acetophenone. This synthesis provides several advantages such as excellent yields of the required products. The prepared compounds (1-11) were identified by m.p., IR, CHN analysis, 1H ND 13C-NMR

AB - Dowex-50W-sodium ion exchange was used after acidification and modification via nitration and sulfonation as a reusable catalyst for the synthesis of chalcones containing hydroxyl and nitro groups through condensation of substituted aldehydes and substituted acetophenone. This synthesis provides several advantages such as excellent yields of the required products. The prepared compounds (1-11) were identified by m.p., IR, CHN analysis, 1H ND 13C-NMR

KW - Dowex resin

KW - chalcones

KW - Claisen-Schmidt condensation

UR - http://www.journals.elsevier.com/karbala-international-journal-of-modern-science

U2 - 10.1016/j.kijoms.2014.12.001

DO - 10.1016/j.kijoms.2014.12.001

M3 - Article

JO - Karbala International Journal of Modern Science

JF - Karbala International Journal of Modern Science

ER -

Modified dowex-50 W-promoted synthesis of chalcones containing hydroxyl and nitro groups

Abstract

Keywords

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