Extraction of benzene, toluene, ethyl benzene, xylene and cumene from soil using methanol at elevated temperature and pressure

Kate M Meney, Christine M. Davidson, David Littlejohn, Nicholas J. Cotton, Bernard Fields

Research output: Contribution to journalArticle

3 Citations (Scopus)

Abstract

A system for solvent extraction at elevated temperature and pressure has been constructed from parts of HPLC and GC instruments, The apparatus has been used successfully to remove benzene, toluene, ethyl benzene, p-xylene and cumene from vapour-fortified clay soil, Quantitative recoveries (100 +/- 10%) were obtained for all analytes, provided the collection vial was cooled to around -3 degrees C in an ice-salt mixture, When the performance was compared with that of a commercial, accelerated solvent extraction system, similar levels of ethyl benzene, p-xylene and cumene were extracted, However, the recoveries and, in particular, the reproducibility were significantly better for benzene and toluene with the system developed.

LanguageEnglish
Pages173-175
Number of pages3
JournalAnalytical Communications
Volume35
Issue number6
DOIs
Publication statusPublished - Jun 1998

Fingerprint

Xylenes
Ethylbenzene
Toluene
Solvent extraction
Benzene
Methanol
Soils
Recovery
Ice
Salts
Vapors
Temperature
4-xylene
cumene
clay

Keywords

  • elevated temperature
  • solvent extraction
  • vapour-fortified clay soil

Cite this

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title = "Extraction of benzene, toluene, ethyl benzene, xylene and cumene from soil using methanol at elevated temperature and pressure",
abstract = "A system for solvent extraction at elevated temperature and pressure has been constructed from parts of HPLC and GC instruments, The apparatus has been used successfully to remove benzene, toluene, ethyl benzene, p-xylene and cumene from vapour-fortified clay soil, Quantitative recoveries (100 +/- 10{\%}) were obtained for all analytes, provided the collection vial was cooled to around -3 degrees C in an ice-salt mixture, When the performance was compared with that of a commercial, accelerated solvent extraction system, similar levels of ethyl benzene, p-xylene and cumene were extracted, However, the recoveries and, in particular, the reproducibility were significantly better for benzene and toluene with the system developed.",
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}

Extraction of benzene, toluene, ethyl benzene, xylene and cumene from soil using methanol at elevated temperature and pressure. / Meney, Kate M ; Davidson, Christine M.; Littlejohn, David; Cotton, Nicholas J. ; Fields, Bernard.

In: Analytical Communications , Vol. 35, No. 6, 06.1998, p. 173-175.

Research output: Contribution to journalArticle

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T1 - Extraction of benzene, toluene, ethyl benzene, xylene and cumene from soil using methanol at elevated temperature and pressure

AU - Meney, Kate M

AU - Davidson, Christine M.

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AU - Cotton, Nicholas J.

AU - Fields, Bernard

PY - 1998/6

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KW - solvent extraction

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