Designing a TiO2-MoO3-BMIMBr nanocomposite by a solvohydrothermal method using an ionic liquid aqueous mixture: an ultra high sensitive acetaminophen sensor

Anita K. Tawade; Ajay P. Khairnar; Jayashri V. Kamble; Akash R. Kadam; Kiran Kumar K. Sharma; Anil A. Powar; Vijay S. Patil; Manohar R. Patil; Sawanta S. Mali; Chang Kook Hong; Shivaji N. Tayade

doi:10.1039/D3RA02611F

Designing a TiO2-MoO3-BMIMBr nanocomposite by a solvohydrothermal method using an ionic liquid aqueous mixture: an ultra high sensitive acetaminophen sensor

Anita K. Tawade, Ajay P. Khairnar, Jayashri V. Kamble, Akash R. Kadam, Kiran Kumar K. Sharma, Anil A. Powar, Vijay S. Patil, Manohar R. Patil^*, Sawanta S. Mali, Chang Kook Hong, Shivaji N. Tayade^*

^*Corresponding author for this work

Pure And Applied Chemistry

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Abstract

This study shows a simplistic, efficient procedure to synthesize TiO2-MoO3-BMIMBr nanocomposites. Powder X-ray diffraction, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray photoelectron spectroscopy have all been used to completely analyse the materials. The detection of acetaminophen (AC) has been examined at a modified glassy carbon electrode with TiO2-MoO3-BMIMBr nanocomposites. Moreover, the electrochemical behavior of the nanocomposite modified electrode has been studied by cyclic voltammetry (CV), differential pulse voltammetry (DPV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The linear response of AC was observed in the range 8.26–124.03 nM. The sensitivity and detection limits (S/N = 3) were found to be 1.16 μA L mol−1 cm−2 and 11.54 nM by CV and 24 μA L mol−1 cm−2 and 8.16 nM by DPV respectively.

Original language	English
Pages (from-to)	21283-21295
Number of pages	13
Journal	RSC Advances
Volume	13
Issue number	31
DOIs	https://doi.org/10.1039/D3RA02611F
Publication status	Published - 14 Jul 2023

Keywords

pharmaceutical industry
acetaminophen
electrochemical sensing platform

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10.1039/D3RA02611FLicence: CC BY 3.0

Tawade-etal-RSCA-2023-Designing-a-TiO2-MoO3-BMIMBr-nanocomposite-by-a-solvohydrothermal-method-using-an-ionic-liquidFinal published version, 1.8 MBLicence: CC BY 3.0

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Tawade, A. K., Khairnar, A. P., Kamble, J. V., Kadam, A. R., Sharma, K. K. K., Powar, A. A., Patil, V. S., Patil, M. R., Mali, S. S., Hong, C. K., & Tayade, S. N. (2023). Designing a TiO2-MoO3-BMIMBr nanocomposite by a solvohydrothermal method using an ionic liquid aqueous mixture: an ultra high sensitive acetaminophen sensor. RSC Advances, 13(31), 21283-21295. https://doi.org/10.1039/D3RA02611F

@article{73ac040ded394cbda7727c15bed5600a,

title = "Designing a TiO2-MoO3-BMIMBr nanocomposite by a solvohydrothermal method using an ionic liquid aqueous mixture: an ultra high sensitive acetaminophen sensor",

abstract = "This study shows a simplistic, efficient procedure to synthesize TiO2-MoO3-BMIMBr nanocomposites. Powder X-ray diffraction, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray photoelectron spectroscopy have all been used to completely analyse the materials. The detection of acetaminophen (AC) has been examined at a modified glassy carbon electrode with TiO2-MoO3-BMIMBr nanocomposites. Moreover, the electrochemical behavior of the nanocomposite modified electrode has been studied by cyclic voltammetry (CV), differential pulse voltammetry (DPV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The linear response of AC was observed in the range 8.26–124.03 nM. The sensitivity and detection limits (S/N = 3) were found to be 1.16 μA L mol−1 cm−2 and 11.54 nM by CV and 24 μA L mol−1 cm−2 and 8.16 nM by DPV respectively.",

keywords = "pharmaceutical industry, acetaminophen, electrochemical sensing platform",

author = "Tawade, {Anita K.} and Khairnar, {Ajay P.} and Kamble, {Jayashri V.} and Kadam, {Akash R.} and Sharma, {Kiran Kumar K.} and Powar, {Anil A.} and Patil, {Vijay S.} and Patil, {Manohar R.} and Mali, {Sawanta S.} and Hong, {Chang Kook} and Tayade, {Shivaji N.}",

year = "2023",

month = jul,

day = "14",

doi = "10.1039/D3RA02611F",

language = "English",

volume = "13",

pages = "21283--21295",

journal = "RSC Advances",

issn = "2046-2069",

publisher = "Royal Society of Chemistry",

number = "31",

}

Tawade, AK, Khairnar, AP, Kamble, JV, Kadam, AR, Sharma, KKK, Powar, AA, Patil, VS, Patil, MR, Mali, SS, Hong, CK & Tayade, SN 2023, 'Designing a TiO2-MoO3-BMIMBr nanocomposite by a solvohydrothermal method using an ionic liquid aqueous mixture: an ultra high sensitive acetaminophen sensor', RSC Advances, vol. 13, no. 31, pp. 21283-21295. https://doi.org/10.1039/D3RA02611F

TY - JOUR

T1 - Designing a TiO2-MoO3-BMIMBr nanocomposite by a solvohydrothermal method using an ionic liquid aqueous mixture: an ultra high sensitive acetaminophen sensor

AU - Tawade, Anita K.

AU - Khairnar, Ajay P.

AU - Kamble, Jayashri V.

AU - Kadam, Akash R.

AU - Sharma, Kiran Kumar K.

AU - Powar, Anil A.

AU - Patil, Vijay S.

AU - Patil, Manohar R.

AU - Mali, Sawanta S.

AU - Hong, Chang Kook

AU - Tayade, Shivaji N.

PY - 2023/7/14

Y1 - 2023/7/14

N2 - This study shows a simplistic, efficient procedure to synthesize TiO2-MoO3-BMIMBr nanocomposites. Powder X-ray diffraction, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray photoelectron spectroscopy have all been used to completely analyse the materials. The detection of acetaminophen (AC) has been examined at a modified glassy carbon electrode with TiO2-MoO3-BMIMBr nanocomposites. Moreover, the electrochemical behavior of the nanocomposite modified electrode has been studied by cyclic voltammetry (CV), differential pulse voltammetry (DPV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The linear response of AC was observed in the range 8.26–124.03 nM. The sensitivity and detection limits (S/N = 3) were found to be 1.16 μA L mol−1 cm−2 and 11.54 nM by CV and 24 μA L mol−1 cm−2 and 8.16 nM by DPV respectively.

AB - This study shows a simplistic, efficient procedure to synthesize TiO2-MoO3-BMIMBr nanocomposites. Powder X-ray diffraction, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray photoelectron spectroscopy have all been used to completely analyse the materials. The detection of acetaminophen (AC) has been examined at a modified glassy carbon electrode with TiO2-MoO3-BMIMBr nanocomposites. Moreover, the electrochemical behavior of the nanocomposite modified electrode has been studied by cyclic voltammetry (CV), differential pulse voltammetry (DPV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The linear response of AC was observed in the range 8.26–124.03 nM. The sensitivity and detection limits (S/N = 3) were found to be 1.16 μA L mol−1 cm−2 and 11.54 nM by CV and 24 μA L mol−1 cm−2 and 8.16 nM by DPV respectively.

KW - pharmaceutical industry

KW - acetaminophen

KW - electrochemical sensing platform

U2 - 10.1039/D3RA02611F

DO - 10.1039/D3RA02611F

M3 - Article

SN - 2046-2069

VL - 13

SP - 21283

EP - 21295

JO - RSC Advances

JF - RSC Advances

IS - 31

ER -

Designing a TiO2-MoO3-BMIMBr nanocomposite by a solvohydrothermal method using an ionic liquid aqueous mixture: an ultra high sensitive acetaminophen sensor

Abstract

Keywords

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