Cytenamide-formic acid (1/1)

A. Johnston; A.J. Florence; Gary J. Miller; A.R. Kennedy; Colin T. Bedford

doi:10.1107/S1600536808019181

Cytenamide-formic acid (1/1)

A. Johnston, A.J. Florence, Gary J. Miller, A.R. Kennedy, Colin T. Bedford

Research output: Contribution to journal › Article › peer-review

2 Citations (Scopus)

Abstract

In the crystal structure of the title compound [systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide-methanoic acid (1/1)], C16H13NO·CH2O2, the cytenamide and solvent molecules form a hydrogen-bonded R22(8) dimer motif, which is further connected to form a centrosymmetric double-motif arrangement. The asymmetric unit contains two formula units.

Original language	English
Pages (from-to)	1379-1380
Number of pages	1
Journal	Acta Crystallographica Section E: Structure Reports
Volume	64
DOIs	https://doi.org/10.1107/S1600536808019181
Publication status	Published - Aug 2008

Keywords

single-crystal X-ray study
T = 123 K
mean (C–C) = 0.001 A°
R factor = 0.047
wR factor = 0.142
data-to-parameter ratio = 31.6.

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10.1107/S1600536808019181

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@article{60163bba9faa456db3977bdd76e280da,

title = "Cytenamide-formic acid (1/1)",

abstract = "In the crystal structure of the title compound [systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide-methanoic acid (1/1)], C16H13NO·CH2O2, the cytenamide and solvent molecules form a hydrogen-bonded R22(8) dimer motif, which is further connected to form a centrosymmetric double-motif arrangement. The asymmetric unit contains two formula units.",

keywords = "single-crystal X-ray study, T = 123 K, mean (C–C) = 0.001 A°, R factor = 0.047, wR factor = 0.142, data-to-parameter ratio = 31.6.",

author = "A. Johnston and A.J. Florence and Miller, \{Gary J.\} and A.R. Kennedy and Bedford, \{Colin T.\}",

year = "2008",

month = aug,

doi = "10.1107/S1600536808019181",

language = "English",

volume = "64",

pages = "1379--1380",

journal = "Acta Crystallographica Section E: Structure Reports",

issn = "1600-5368",

}

TY - JOUR

T1 - Cytenamide-formic acid (1/1)

AU - Johnston, A.

AU - Florence, A.J.

AU - Miller, Gary J.

AU - Kennedy, A.R.

AU - Bedford, Colin T.

PY - 2008/8

Y1 - 2008/8

N2 - In the crystal structure of the title compound [systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide-methanoic acid (1/1)], C16H13NO·CH2O2, the cytenamide and solvent molecules form a hydrogen-bonded R22(8) dimer motif, which is further connected to form a centrosymmetric double-motif arrangement. The asymmetric unit contains two formula units.

AB - In the crystal structure of the title compound [systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide-methanoic acid (1/1)], C16H13NO·CH2O2, the cytenamide and solvent molecules form a hydrogen-bonded R22(8) dimer motif, which is further connected to form a centrosymmetric double-motif arrangement. The asymmetric unit contains two formula units.

KW - single-crystal X-ray study

KW - T = 123 K

KW - mean (C–C) = 0.001 A°

KW - R factor = 0.047

KW - wR factor = 0.142

KW - data-to-parameter ratio = 31.6.

UR - http://dx.doi.org/10.1107/S1600536808019181

U2 - 10.1107/S1600536808019181

DO - 10.1107/S1600536808019181

M3 - Article

SN - 1600-5368

VL - 64

SP - 1379

EP - 1380

JO - Acta Crystallographica Section E: Structure Reports

JF - Acta Crystallographica Section E: Structure Reports

ER -

Cytenamide-formic acid (1/1)

Abstract

Keywords

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Physical Organic Chemistry: Opportunities In Synthesis, Materials And Pharmaceuticals (Science And Innovation Award)

x-ray diffractometer

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Cytenamide-formic acid (1/1)

Abstract

Keywords

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Projects

Physical Organic Chemistry: Opportunities In Synthesis, Materials And Pharmaceuticals (Science And Innovation Award)

Equipment

x-ray diffractometer

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