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In the crystal structure of the title compound (systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide ethanoic acid solvate), C16H13NO·C2H4O2, the cytenamide and solvent molecules form a hydrogen-bonded R22(8) dimer motif, which is further connected to form a centrosymmetric double ring motif arrangement. The cycloheptene ring adopts a boat conformation and the dihedral angle between the least-squares planes through the two aromatic rings is 54.7 (2)°.
|Number of pages||1|
|Journal||Acta Crystallographica Section E: Structure Reports|
|Publication status||Published - Jun 2008|
- single-crystal X-ray study
- T = 160 K
- mean (C–C) = 0.006 A°
- R factor = 0.090
- wR factor = 0.148
- data-to-parameter ratio = 13.9
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