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The mixed solvated salt 4-(2-chlorodibenzo[b,f][1,4]oxazepin-11-yl)piperazin-1-ium acetate-acetic acid-cyclohexane (2/2/1), C17H17ClN3O+·C2H3O2-·C2H4O2·0.5C6H12, crystallizes with one molecule of protonated amoxapine (AXPN), an acetate anion and a molecule of acetic acid together with half a molecule of cyclohexane. In the centrosymmetric crystal, both enantiomers of the protonated AXPN molecule stack alternatively along . Acetate anions connect the AXPN cations through N-H...O hydrogen bonding in the  direction, creating a sheet lying parallel to (100). The acetic acid molecules are linked to the acetate anions via O-H...O hydrogen bonds within the sheets. Within the sheets there are also a number of C-H...O hydrogen bonds present. The cyclohexane solvent molecules occupy the space between the sheets.
|Number of pages||3|
|Journal||Acta Crystallographica Section E: Structure Reports|
|Publication status||Published - 1 Feb 2015|
- crystal structure
- hydrogen bonding
- mixed solvate