Crystal structure of 2-nitro-N-(2-nitrophenyl)benzamide

R. Moreno-Fuquen, A. Azcárate, A. R. Kennedy

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Abstract

In the title compound, C13H9N3O5, the mean plane of the non-H atoms of the central amide fragment C—N—C( O)—C [r.m.s. deviation = 0.0442 A ˚ ] forms dihedral angles of 71.76 (6) and 24.29 (10) with the C-bonded and N-bonded benzene rings, respectively. In the crystal, molecules are linked by N—H O hydrogen bonds forming C(4) chains along [100].Weak C—H O contacts link the molecules into (100) sheets containing edge-fused R4 4(30) rings. Together, the N—H O and C—H O hydrogen bonds generate a three-dimensional network.
Original languageEnglish
Pages (from-to)o389-o390
Number of pages2
JournalActa Crystallographica Section E: Structure Reports
Volume71
Issue number6
Early online date9 May 2015
DOIs
Publication statusPublished - Jun 2015

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Hydrogen bonds
Crystal structure
methylidyne
hydrogen bonds
crystal structure
Molecules
rings
Dihedral angle
Benzene
Amides
amides
dihedral angle
molecules
benzene
fragments
deviation
Atoms
Crystals
crystals
atoms

Keywords

  • non-H atoms
  • hydrogen bonds
  • crystal molecules

Cite this

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Crystal structure of 2-nitro-N-(2-nitrophenyl)benzamide. / Moreno-Fuquen, R.; Azcárate, A.; Kennedy, A. R.

In: Acta Crystallographica Section E: Structure Reports, Vol. 71, No. 6, 06.2015, p. o389-o390.

Research output: Contribution to journalArticle

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T1 - Crystal structure of 2-nitro-N-(2-nitrophenyl)benzamide

AU - Moreno-Fuquen, R.

AU - Azcárate, A.

AU - Kennedy, A. R.

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Y1 - 2015/6

N2 - In the title compound, C13H9N3O5, the mean plane of the non-H atoms of the central amide fragment C—N—C( O)—C [r.m.s. deviation = 0.0442 A ˚ ] forms dihedral angles of 71.76 (6) and 24.29 (10) with the C-bonded and N-bonded benzene rings, respectively. In the crystal, molecules are linked by N—H O hydrogen bonds forming C(4) chains along [100].Weak C—H O contacts link the molecules into (100) sheets containing edge-fused R4 4(30) rings. Together, the N—H O and C—H O hydrogen bonds generate a three-dimensional network.

AB - In the title compound, C13H9N3O5, the mean plane of the non-H atoms of the central amide fragment C—N—C( O)—C [r.m.s. deviation = 0.0442 A ˚ ] forms dihedral angles of 71.76 (6) and 24.29 (10) with the C-bonded and N-bonded benzene rings, respectively. In the crystal, molecules are linked by N—H O hydrogen bonds forming C(4) chains along [100].Weak C—H O contacts link the molecules into (100) sheets containing edge-fused R4 4(30) rings. Together, the N—H O and C—H O hydrogen bonds generate a three-dimensional network.

KW - non-H atoms

KW - hydrogen bonds

KW - crystal molecules

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