Application of triple-channel C-13{H-1,F-19} NMR techniques to probe structural properties of disordered solids

A  Nordon; R K  Harris; L  Yeo; K D M  Harris

doi:10.1039/A705053D

Application of triple-channel C-13{H-1,F-19} NMR techniques to probe structural properties of disordered solids

A Nordon, R K Harris, L Yeo, K D M Harris

Pure And Applied Chemistry

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13 Citations (Scopus)

Abstract

Triple-channel C-13 MAS NMR experiments are carried out to characterize intermolecular interactions in disordered molecular solids containing fluorinated n-alkanes; an approach invoking a combination of H-1 --> C-13 and F-19 --> C-13 cross-polarization experiments, with both single-channel (H-1) and double-channel (H-1,F-19) decoupling is developed to assign resonances for a given type of C-13 nucleus in different intermolecular environments.

Original language	English
Pages (from-to)	2045-2046
Number of pages	2
Journal	Chemical Communications
Issue number	21
DOIs	https://doi.org/10.1039/A705053D
Publication status	Published - 7 Nov 1997

Keywords

functional-group recognition
inclusion-compounds

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10.1039/A705053D

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title = "Application of triple-channel C-13{H-1,F-19} NMR techniques to probe structural properties of disordered solids",

abstract = "Triple-channel C-13 MAS NMR experiments are carried out to characterize intermolecular interactions in disordered molecular solids containing fluorinated n-alkanes; an approach invoking a combination of H-1 --> C-13 and F-19 --> C-13 cross-polarization experiments, with both single-channel (H-1) and double-channel (H-1,F-19) decoupling is developed to assign resonances for a given type of C-13 nucleus in different intermolecular environments.",

keywords = "functional-group recognition, inclusion-compounds",

author = "A Nordon and Harris, {R K} and L Yeo and Harris, {K D M}",

year = "1997",

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AU - Nordon, A

AU - Harris, R K

AU - Yeo, L

AU - Harris, K D M

PY - 1997/11/7

Y1 - 1997/11/7

N2 - Triple-channel C-13 MAS NMR experiments are carried out to characterize intermolecular interactions in disordered molecular solids containing fluorinated n-alkanes; an approach invoking a combination of H-1 --> C-13 and F-19 --> C-13 cross-polarization experiments, with both single-channel (H-1) and double-channel (H-1,F-19) decoupling is developed to assign resonances for a given type of C-13 nucleus in different intermolecular environments.

AB - Triple-channel C-13 MAS NMR experiments are carried out to characterize intermolecular interactions in disordered molecular solids containing fluorinated n-alkanes; an approach invoking a combination of H-1 --> C-13 and F-19 --> C-13 cross-polarization experiments, with both single-channel (H-1) and double-channel (H-1,F-19) decoupling is developed to assign resonances for a given type of C-13 nucleus in different intermolecular environments.

KW - functional-group recognition

KW - inclusion-compounds

U2 - 10.1039/A705053D

DO - 10.1039/A705053D

M3 - Article

SP - 2045

EP - 2046

JO - Chemical Communications

JF - Chemical Communications

SN - 1359-7345

IS - 21

ER -

Application of triple-channel C-13{H-1,F-19} NMR techniques to probe structural properties of disordered solids

Abstract

Keywords

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