Application of triple-channel C-13{H-1,F-19} NMR techniques to probe structural properties of disordered solids

A Nordon, R K Harris, L Yeo, K D M Harris

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Abstract

Triple-channel C-13 MAS NMR experiments are carried out to characterize intermolecular interactions in disordered molecular solids containing fluorinated n-alkanes; an approach invoking a combination of H-1 --> C-13 and F-19 --> C-13 cross-polarization experiments, with both single-channel (H-1) and double-channel (H-1,F-19) decoupling is developed to assign resonances for a given type of C-13 nucleus in different intermolecular environments.

Original languageEnglish
Pages (from-to)2045-2046
Number of pages2
JournalChemical Communications
Issue number21
DOIs
Publication statusPublished - 7 Nov 1997

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Keywords

  • functional-group recognition
  • inclusion-compounds

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