A catemer-to-dimer structural transformation in cyheptamide

A.J. Florence, K. Shankland, T. Gelbrich, M.B. Hursthouse, N. Shankland, Andrea Johnston, P. Fernandes, C.K. Leech

Research output: Contribution to journalArticle

27 Citations (Scopus)

Abstract

A catemeric crystal structure of cyheptamide undergoes a transformation in the solid-state upon heating to produce a dimer-based form whose structure has been determined from laboratory X-ray powder diffraction (XRPD) data, thereby providing the first conclusive evidence of a carbamazepine analogue crystallising in both hydrogen bonded motifs.
LanguageEnglish
Pages26-28
Number of pages2
JournalCrystEngComm
Volume10
DOIs
Publication statusPublished - 2008

Fingerprint

Carbamazepine
Dimers
X ray powder diffraction
Hydrogen
Crystal structure
dimers
analogs
solid state
Heating
crystal structure
heating
hydrogen
diffraction
x rays
cyheptamide

Keywords

  • catemer-to-dimer
  • cyheptamide
  • crystallography
  • biomedical sciences

Cite this

Florence, A. J., Shankland, K., Gelbrich, T., Hursthouse, M. B., Shankland, N., Johnston, A., ... Leech, C. K. (2008). A catemer-to-dimer structural transformation in cyheptamide. CrystEngComm, 10, 26-28. https://doi.org/10.1039/b712547j
Florence, A.J. ; Shankland, K. ; Gelbrich, T. ; Hursthouse, M.B. ; Shankland, N. ; Johnston, Andrea ; Fernandes, P. ; Leech, C.K. / A catemer-to-dimer structural transformation in cyheptamide. In: CrystEngComm. 2008 ; Vol. 10. pp. 26-28.
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Florence, AJ, Shankland, K, Gelbrich, T, Hursthouse, MB, Shankland, N, Johnston, A, Fernandes, P & Leech, CK 2008, 'A catemer-to-dimer structural transformation in cyheptamide' CrystEngComm, vol. 10, pp. 26-28. https://doi.org/10.1039/b712547j

A catemer-to-dimer structural transformation in cyheptamide. / Florence, A.J.; Shankland, K.; Gelbrich, T.; Hursthouse, M.B.; Shankland, N.; Johnston, Andrea; Fernandes, P.; Leech, C.K.

In: CrystEngComm, Vol. 10, 2008, p. 26-28.

Research output: Contribution to journalArticle

TY - JOUR

T1 - A catemer-to-dimer structural transformation in cyheptamide

AU - Florence, A.J.

AU - Shankland, K.

AU - Gelbrich, T.

AU - Hursthouse, M.B.

AU - Shankland, N.

AU - Johnston, Andrea

AU - Fernandes, P.

AU - Leech, C.K.

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AB - A catemeric crystal structure of cyheptamide undergoes a transformation in the solid-state upon heating to produce a dimer-based form whose structure has been determined from laboratory X-ray powder diffraction (XRPD) data, thereby providing the first conclusive evidence of a carbamazepine analogue crystallising in both hydrogen bonded motifs.

KW - catemer-to-dimer

KW - cyheptamide

KW - crystallography

KW - biomedical sciences

UR - http://dx.doi.org/10.1039/b712547j

U2 - 10.1039/b712547j

DO - 10.1039/b712547j

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VL - 10

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JO - CrystEngComm

T2 - CrystEngComm

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SN - 1466-8033

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Florence AJ, Shankland K, Gelbrich T, Hursthouse MB, Shankland N, Johnston A et al. A catemer-to-dimer structural transformation in cyheptamide. CrystEngComm. 2008;10:26-28. https://doi.org/10.1039/b712547j