3,4-Dichloro-1-nitro­benzene-1,4-dioxane (4/1)

S.A. Barnett; A. Johnston; A.J. Florence; A.R. Kennedy

doi:10.1107/S1600536805030680

3,4-Dichloro-1-nitrobenzene-1,4-dioxane (4/1)

S.A. Barnett, A. Johnston, A.J. Florence, A.R. Kennedy

Research output: Contribution to journal › Article › peer-review

3 Citations (Scopus)

Abstract

The solvate structure of 3,4-dichloro-1-nitrobenzene with 1,4-dioxane, C6H3Cl2NO2·0.25C4H8N2, is reported. The asymmetric unit comprises two independent 3,4-dichloro-1-nitrobenzene molecules and half of a 1,4-dioxane molecule, the solvent molecule being disposed about a centre of inversion. Double chains of 3,4-dichloro-1-nitrobenzene are linked by ClCl interactions and 1,4-dioxane molecules via C - HO hydrogen bonds into a two-dimensional sheet.

Original language	English
Pages (from-to)	o3666-o3667
Journal	Acta Crystallographica Section E: Structure Reports
Volume	61
Issue number	11
DOIs	https://doi.org/10.1107/S1600536805030680
Publication status	Published - Nov 2005

Keywords

nitrobenzene molecules
dioxane
hydrogen bonds
two-dimensional

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10.1107/S1600536805030680

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title = "3,4-Dichloro-1-nitrobenzene-1,4-dioxane (4/1)",

abstract = "The solvate structure of 3,4-dichloro-1-nitrobenzene with 1,4-dioxane, C6H3Cl2NO2·0.25C4H8N2, is reported. The asymmetric unit comprises two independent 3,4-dichloro-1-nitrobenzene molecules and half of a 1,4-dioxane molecule, the solvent molecule being disposed about a centre of inversion. Double chains of 3,4-dichloro-1-nitrobenzene are linked by ClCl interactions and 1,4-dioxane molecules via C - HO hydrogen bonds into a two-dimensional sheet.",

keywords = "nitrobenzene molecules, dioxane, hydrogen bonds, two-dimensional",

author = "S.A. Barnett and A. Johnston and A.J. Florence and A.R. Kennedy",

year = "2005",

month = nov,

doi = "10.1107/S1600536805030680",

language = "English",

volume = "61",

pages = "o3666--o3667",

journal = "Acta Crystallographica Section E: Structure Reports",

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TY - JOUR

T1 - 3,4-Dichloro-1-nitrobenzene-1,4-dioxane (4/1)

AU - Barnett, S.A.

AU - Johnston, A.

AU - Florence, A.J.

AU - Kennedy, A.R.

PY - 2005/11

Y1 - 2005/11

N2 - The solvate structure of 3,4-dichloro-1-nitrobenzene with 1,4-dioxane, C6H3Cl2NO2·0.25C4H8N2, is reported. The asymmetric unit comprises two independent 3,4-dichloro-1-nitrobenzene molecules and half of a 1,4-dioxane molecule, the solvent molecule being disposed about a centre of inversion. Double chains of 3,4-dichloro-1-nitrobenzene are linked by ClCl interactions and 1,4-dioxane molecules via C - HO hydrogen bonds into a two-dimensional sheet.

AB - The solvate structure of 3,4-dichloro-1-nitrobenzene with 1,4-dioxane, C6H3Cl2NO2·0.25C4H8N2, is reported. The asymmetric unit comprises two independent 3,4-dichloro-1-nitrobenzene molecules and half of a 1,4-dioxane molecule, the solvent molecule being disposed about a centre of inversion. Double chains of 3,4-dichloro-1-nitrobenzene are linked by ClCl interactions and 1,4-dioxane molecules via C - HO hydrogen bonds into a two-dimensional sheet.

KW - nitrobenzene molecules

KW - dioxane

KW - hydrogen bonds

KW - two-dimensional

UR - http://dx.doi.org/10.1107/S1600536805030680

U2 - 10.1107/S1600536805030680

DO - 10.1107/S1600536805030680

M3 - Article

SN - 1600-5368

VL - 61

SP - o3666-o3667

JO - Acta Crystallographica Section E: Structure Reports

JF - Acta Crystallographica Section E: Structure Reports

IS - 11

ER -

3,4-Dichloro-1-nitrobenzene-1,4-dioxane (4/1)

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3,4-Dichloro-1-nitro­benzene-1,4-dioxane (4/1)

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3,4-Dichloro-1-nitrobenzene-1,4-dioxane (4/1)