3,4-Dichloro-1-nitro­benzene-1,4-dioxane (4/1)

S.A. Barnett, A. Johnston, A.J. Florence, A.R. Kennedy

Research output: Contribution to journalArticle

3 Citations (Scopus)

Abstract

The solvate structure of 3,4-dichloro-1-nitro­benzene with 1,4-dioxane, C6H3Cl2NO2·0.25C4H8N2, is reported. The asymmetric unit comprises two independent 3,4-dichloro-1-nitro­benzene mol­ecules and half of a 1,4-dioxane mol­ecule, the solvent molecule being disposed about a centre of inversion. Double chains of 3,4-dichloro-1-nitro­benzene are linked by ClCl inter­actions and 1,4-dioxane mol­ecules via C - HO hydrogen bonds into a two-dimensional sheet.
Original languageEnglish
Pages (from-to)o3666-o3667
JournalActa Crystallographica Section E: Structure Reports
Volume61
Issue number11
DOIs
Publication statusPublished - Nov 2005

Fingerprint

Nitrobenzene
nitrobenzenes
Molecules
molecules
Hydrogen bonds
inversions
hydrogen bonds
nitrobenzene
1,4-dioxane
interactions

Keywords

  • nitrobenzene molecules
  • dioxane
  • hydrogen bonds
  • two-dimensional

Cite this

@article{265763daf919416083873d9086daace6,
title = "3,4-Dichloro-1-nitro­benzene-1,4-dioxane (4/1)",
abstract = "The solvate structure of 3,4-dichloro-1-nitro­benzene with 1,4-dioxane, C6H3Cl2NO2·0.25C4H8N2, is reported. The asymmetric unit comprises two independent 3,4-dichloro-1-nitro­benzene mol­ecules and half of a 1,4-dioxane mol­ecule, the solvent molecule being disposed about a centre of inversion. Double chains of 3,4-dichloro-1-nitro­benzene are linked by ClCl inter­actions and 1,4-dioxane mol­ecules via C - HO hydrogen bonds into a two-dimensional sheet.",
keywords = "nitrobenzene molecules, dioxane, hydrogen bonds, two-dimensional",
author = "S.A. Barnett and A. Johnston and A.J. Florence and A.R. Kennedy",
year = "2005",
month = "11",
doi = "10.1107/S1600536805030680",
language = "English",
volume = "61",
pages = "o3666--o3667",
journal = "Acta Crystallographica Section E: Structure Reports",
issn = "1600-5368",
number = "11",

}

3,4-Dichloro-1-nitro­benzene-1,4-dioxane (4/1). / Barnett, S.A.; Johnston, A.; Florence, A.J.; Kennedy, A.R.

In: Acta Crystallographica Section E: Structure Reports, Vol. 61, No. 11, 11.2005, p. o3666-o3667.

Research output: Contribution to journalArticle

TY - JOUR

T1 - 3,4-Dichloro-1-nitro­benzene-1,4-dioxane (4/1)

AU - Barnett, S.A.

AU - Johnston, A.

AU - Florence, A.J.

AU - Kennedy, A.R.

PY - 2005/11

Y1 - 2005/11

N2 - The solvate structure of 3,4-dichloro-1-nitro­benzene with 1,4-dioxane, C6H3Cl2NO2·0.25C4H8N2, is reported. The asymmetric unit comprises two independent 3,4-dichloro-1-nitro­benzene mol­ecules and half of a 1,4-dioxane mol­ecule, the solvent molecule being disposed about a centre of inversion. Double chains of 3,4-dichloro-1-nitro­benzene are linked by ClCl inter­actions and 1,4-dioxane mol­ecules via C - HO hydrogen bonds into a two-dimensional sheet.

AB - The solvate structure of 3,4-dichloro-1-nitro­benzene with 1,4-dioxane, C6H3Cl2NO2·0.25C4H8N2, is reported. The asymmetric unit comprises two independent 3,4-dichloro-1-nitro­benzene mol­ecules and half of a 1,4-dioxane mol­ecule, the solvent molecule being disposed about a centre of inversion. Double chains of 3,4-dichloro-1-nitro­benzene are linked by ClCl inter­actions and 1,4-dioxane mol­ecules via C - HO hydrogen bonds into a two-dimensional sheet.

KW - nitrobenzene molecules

KW - dioxane

KW - hydrogen bonds

KW - two-dimensional

UR - http://dx.doi.org/10.1107/S1600536805030680

U2 - 10.1107/S1600536805030680

DO - 10.1107/S1600536805030680

M3 - Article

VL - 61

SP - o3666-o3667

JO - Acta Crystallographica Section E: Structure Reports

JF - Acta Crystallographica Section E: Structure Reports

SN - 1600-5368

IS - 11

ER -