Abstract
The nitration of 1-(triisopropylsilyl)-1H-pyrrole leads to a mixt. of products following partial acid cleavage of the triisopropylsilyl protecting group. Structural detn. showed the isolated products to be 3-nitro-1-(triisopropylsilyl)-1H-pyrrole, C13H24N2O2Si (I), and 2,4-dinitropyrrole. In the solid state, I exists as discrete mols. with only weak C-H...nitro H bonds between them. Crystallog. data are given.
Original language | English |
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Pages (from-to) | o3282-o3284 |
Number of pages | 3 |
Journal | Acta Crystallographica Section E: Structure Reports |
Volume | 62 |
Issue number | 8 |
DOIs | |
Publication status | Published - Aug 2006 |
Keywords
- nitration
- 4-dinitropyrrole
- hydrogen bonds