3-Nitro-1-(triisopropylsilyl)-1H-pyrrole

Alan Kennedy, Abedawn I. Khalaf, Colin J. Suckling, Roger D. Waigh

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Abstract

The nitration of 1-(triisopropylsilyl)-1H-pyrrole leads to a mixt. of products following partial acid cleavage of the triisopropylsilyl protecting group. Structural detn. showed the isolated products to be 3-nitro-1-(triisopropylsilyl)-1H-pyrrole, C13H24N2O2Si (I), and 2,4-dinitropyrrole. In the solid state, I exists as discrete mols. with only weak C-H...nitro H bonds between them. Crystallog. data are given.
Original languageEnglish
Pages (from-to)o3282-o3284
Number of pages3
JournalActa Crystallographica Section E: Structure Reports
Volume62
Issue number8
DOIs
Publication statusPublished - Aug 2006

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Keywords

  • nitration
  • 4-dinitropyrrole
  • hydrogen bonds

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