The data set contains six files. These data relate to the research reported in the manuscript "Lithium Dihydropyridine Dehydrogenation Catalysis: A Group 1 Approach to Cyclisation of Diamine-Boranes".
The work was carried out in relation to EPSRC grant EP/L027313/1 -
Activated Anionic Aluminium For Synthetic Design, Catalytic and Energy Storage Applications (PI: Dr Stuart D Robertson)
1. Synthetic procedures
2. NMR data (zip file)
3 and 4. Crystallographic information file (X-ray crystallographic data)
5 and 6. CIFcheck (for X-ray crystallographic data)
Note that the NMR data in file 2 contains raw data which requires a specialist program such as Topspin or Mestrelab; and the cif file (file 3) requires a program such as Diamond or Mercury to view.
A temporary embargo has been placed on access to the dataset pending publication.